Molecular Distillation Services/Contract Manufacturing Distillation

TMC performs contract vacuum distillation. Using molecular distillation as an intermediate or final step in the processing of edible oils, waxes or specialty chemicals has added value to our clients products since 1982.

	Flavors and Neutraceuticals TMC has the expertise to provide pure seperations of many oils and food flavorings. The short path, thin film separation process provides a gentle and proven method of purifying and fractionating essential oils. Many flavors can be separated using molecular distillation without danger of oxidation decomposition to provide the highest quality products available. Tolling Profile Sheet
	Specialty Chemicals Your chemicals polymerize or react at normal distillation temperatures and pressures. Using TMC's technology of molecular distillation, the most sensitive of materials will not undergo change and separation can be done efficiently and economically. Purities can be checked on our GC or UV-VIS analytical equipment for the utmost control of quality. Tolling Profile Sheet
	Resins and Synthetic Oils Synthetic oils and resins can be purified on our short path distillation equipment. We can remove odor, reaction by-products and colors to provide the best product attainable. TMC has worked with silicones, perfluoropolyethers, chlorotrifluoroethylenes and many other natural and synthetic polymers. Tolling Profile Sheet
	Wax Products TMC has distilled many wax products. Normally waxes are difficult to distill as they are solids at room temperatures and distill at high temperatures which can be a problem unless the residence time is of short duration. We are experienced in the processing of both low and high temperature wax products and the problems involved using molecular distillation. Tolling Profile Sheet
	Fragrance Industry Using either our molecular distillation or medium vacuum distillation we can purify many of your products. We have experience with a number of fragrances both solids and liquids at room temperature. Eliminate any decomposition and maintain the purity and fragrance you desire. Tolling Profile Sheet

Production Facility

Macro-36 Centrifugal Molecular Stills

Macro-36 CMS stills (centrifugal molecular stills) are capable of distilling up to 400lbs/hr. and are short path thin film. Each has 7 s.f. of evaporating surface and can achieve a vacuum of 5-10 microns giving the following advantages over conventional processing:

Low residence time and therefore minimum thermal hazard to decomposition;
Low temperature distillation of high boilers;
Vacuum deodorization of high molecular weight oils, fats and waxes;
Removal of color bodies;
Removal of reactant components to improve shelf life.
Pilot Molecular Distillation Service

Pilot Molecular Distillation to develop processes and for low volume production.

• Short path thin film distillation.
• Low cost process development.
• Easy to expand to volume on
  CMS-36 stills.
• Development done by experienced   Chemical Engineers.
• Experienced with many chemicals,
   neutraceuticals, fragrances
   & flavors .

Medium Vacuum Distillation

TMC has been doing medium vacuum and atmospheric
distillation of many specialty chemicals such as
perfluorocarbons for the last 20 years.

Applications

Applications of Centrifugal Molecular Stills (CMS)

                     Material                                    Objective                           Results

Citrus Residues

Remove oil from wax

90+% oil recovery

Esters, Fatty Acids

Separate mono - from polyesters

Up to 90+% purity

Specialty Chemicals

Remove color

Remove odor

Color to <2 Gardner

Odorless

Aromatic hydrocarbon chlorinated

95-99% recovery

95% purity

Silicones, Siloxanes

Remove low molecular weights

to 99% purity

Polymers

Remove low molecular weights

to 99% purity

Flavors/Fragrances

Concentrate flavor/fragrances

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Add value to product
Pilot R&D distillation
Production to 2500#/hr
200-5000 molecular weight
Heat sensitive & high boilers
Create zero trans fatty acids

                                              Tolling Profile Sheet

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